柠檬醛分析方法
分析方法
| 方法名称 | 柱型/活性相 | 温度(℃) | 保留指数 (I) | 控温方法 | 备注 | 参考文献 |
|---|---|---|---|---|---|---|
| Kovats' RI, 毛细管柱,等速升温 |
毛细管柱 OV-101
|
-
|
1237.
|
等速升温 |
He, 35. C @ 3. min, 6. K/min; Column length: 12. m; Column diameter: 0.32 mm; Tend: 185. C
|
Marin, A.B.Acree, T.E.Hotchkiss, J.H.Nagy, S.,Gas chromatography--olfactometry of orange juice to assess the effects of plastic polymers on aroma character,J. Agric. Food Chem.,1992, 40, 4, 650-654. 查看文献 |
| Kovats' RI, 填充柱,自定义程序升温 |
填充柱 SE-30
|
-
|
1272.
|
自定义程序升温 |
He, Chromosorb G HP (80-100 mesh); Column length: 1.5 m; Program: not specified
|
Ramsey, J.D.Lee, T.D.Osselton, M.D.Moffat, A.C.,Gas-liquid chromatographic retention indices of 296 non-drug substances on SE-30 or OV-1 likely to be encountered in toxicological analyses,J. Chromatogr.,1980, 184, 2, 185-206. 查看文献 |
| Van Den Dool and Kratz RI, 毛细管柱,等速升温 |
毛细管柱 DB-1
|
-
|
1240.5
|
等速升温 |
2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 300. C
|
Chang, L.P.Sheng, L.S.Yang, M.Z.An, D.K.,Retention index of essential oil in temperature-programmed capillary column gas chromatography,Acta Pharm. Sin.,1989, 24, 11, 847-852. |
| Van Den Dool and Kratz RI, 毛细管柱,等速升温 |
毛细管柱 DB-1
|
-
|
1240.6
|
等速升温 |
2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 300. C
|
Chang, L.P.Sheng, L.S.Yang, M.Z.An, D.K.,Retention index of essential oil in temperature-programmed capillary column gas chromatography,Acta Pharm. Sin.,1989, 24, 11, 847-852. |
| Van Den Dool and Kratz RI, 毛细管柱,等速升温 |
毛细管柱 DB-1
|
-
|
1240.5
|
等速升温 |
2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 300. C
|
Chang, L.P.Sheng, L.S.Yang, M.Z.An, D.K.,Retention index of essential oil in temperature-programmed capillary column gas chromatography,Acta Pharm. Sin.,1989, 24, 11, 847-852. |
| Van Den Dool and Kratz RI, 毛细管柱,等速升温 |
毛细管柱 DB-1
|
-
|
1242.5
|
等速升温 |
2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 300. C
|
Chang, L.P.Sheng, L.S.Yang, M.Z.An, D.K.,Retention index of essential oil in temperature-programmed capillary column gas chromatography,Acta Pharm. Sin.,1989, 24, 11, 847-852. |
| Van Den Dool and Kratz RI, 毛细管柱,等速升温 |
毛细管柱 DB-Wax
|
-
|
1717.5
|
等速升温 |
2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 240. C
|
Chang, L.P.Sheng, L.S.Yang, M.Z.An, D.K.,Retention index of essential oil in temperature-programmed capillary column gas chromatography,Acta Pharm. Sin.,1989, 24, 11, 847-852. |
| Van Den Dool and Kratz RI, 毛细管柱,等速升温 |
毛细管柱 DB-Wax
|
-
|
1720.4
|
等速升温 |
2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 240. C
|
Chang, L.P.Sheng, L.S.Yang, M.Z.An, D.K.,Retention index of essential oil in temperature-programmed capillary column gas chromatography,Acta Pharm. Sin.,1989, 24, 11, 847-852. |
| Van Den Dool and Kratz RI, 毛细管柱,等速升温 |
毛细管柱 DB-Wax
|
-
|
1716.2
|
等速升温 |
2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 240. C
|
Chang, L.P.Sheng, L.S.Yang, M.Z.An, D.K.,Retention index of essential oil in temperature-programmed capillary column gas chromatography,Acta Pharm. Sin.,1989, 24, 11, 847-852. |
| Van Den Dool and Kratz RI, 毛细管柱,等速升温 |
毛细管柱 DB-Wax
|
-
|
1717.5
|
等速升温 |
2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 240. C
|
Chang, L.P.Sheng, L.S.Yang, M.Z.An, D.K.,Retention index of essential oil in temperature-programmed capillary column gas chromatography,Acta Pharm. Sin.,1989, 24, 11, 847-852. |
| Normal alkane RI, 毛细管柱,等速升温 |
毛细管柱 DB-1
|
-
|
1244.
|
等速升温 |
60. m/0.25 mm/0.25 μm, Nitrogen, 60. C @ 1. min, 4. K/min, 250. C @ 10. min
|
Safaei-Ghomi, J.Meshkatalsadat, M.H.Asadi, M.,Analysis of the essential oil of Salvia brachycalyx Boiss. by nano scale injection and antioxidative activity of methanol extract of this plant,Digest J. Nanomaterials and Biostructures,2010, 5, 2, 545-549. |
| Normal alkane RI, 毛细管柱,等速升温 |
毛细管柱 DB-1
|
-
|
1247.
|
等速升温 |
30. m/0.25 mm/0.25 μm, Helium, 50. C @ 2. min, 4. K/min, 220. C @ 2. min
|
Xu, X.Tang, Z.Liang, Y.,Comparative analysis of plant essential oils by GC-MS coupled with integrated chemometric resolution methods,Anal. Methods,2010, 2, 4, 359-367. 查看文献 |
| Normal alkane RI, 毛细管柱,等速升温 |
毛细管柱 SPB-1
|
-
|
1213.
|
等速升温 |
30. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 180. C @ 1. min
|
Kamath, A.Asha, M.R.Ravi, R.Narasimhan, S.Rajalakshmi, D.,Comparative study of odour and GC-olfactometric profiles of selected essential oils,Flavour Fragr. J.,2001, 16, 6, 401-407. 查看文献 |
| Normal alkane RI, 毛细管柱,等速升温 |
毛细管柱 SPB-5
|
-
|
1276.
|
等速升温 |
60. m/0.25 mm/0.25 μm, He, 70. C @ 8. min, 5. K/min, 240. C @ 20. min
|
Kim, H.-J.Kim, K.Kim, N.-S.Lee, D.-S.,Determination of floral fragrances of Rosa hybrida using solid-phase trapping-solvent extraction and gas chromatography-mass spectrometry,J. Chromatogr. A,2000, 902, 2, 389-404. 查看文献 |
| Normal alkane RI, 毛细管柱,自定义程序升温 |
毛细管柱 OV-1
|
-
|
1239.
|
自定义程序升温 |
Helium; Column length: 30. m; Column diameter: 0.25 mm; Program: 40 0C 2 0C/min -> 120 0C 10 0C/min -> 230 0C (15 min)
|
Chen, S.Li, X.,Analysis of common volatile constituents between herbal pair Ephedra Sinica Stapf-Zingiber offoconale Rosc. and its single herb by GC-MS combined with AMWFA method,2011, retrieved from http://www.webmedcentral.com. |
| Normal alkane RI, 毛细管柱,自定义程序升温 |
毛细管柱 DB-1
|
-
|
1216.
|
自定义程序升温 |
30. m/0.25 mm/0.25 μm, Helium; Program: not specified
|
Xu, X.Tang, Z.Liang, Y.,Comparative analysis of plant essential oils by GC-MS coupled with integrated chemometric resolution methods,Anal. Methods,2010, 2, 4, 359-367. 查看文献 |
| Normal alkane RI, 毛细管柱,自定义程序升温 |
毛细管柱 OV-101
|
-
|
1249.
|
自定义程序升温 |
Program: not specified
|
Shibamoto, T.,Retention Indices in Essential Oil Analysis,Capillary Gas Chromatography in Essential Oil Analysis,Sandra, P.; Bicchi, C., ed(s)., Hutchig Verlag, Heidelberg, New York, 1987, 259-274. |
| Normal alkane RI, 其他柱型,自定义程序升温 |
其他柱型 Methyl Silicone
|
-
|
1272.
|
自定义程序升温 |
Program: not specified
|
Ardrey, R.E.Moffat, A.C.,Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase,J. Chromatogr.,1981, 220, 3, 195-252. 查看文献 |
| Normal alkane RI, 毛细管柱,等速升温 |
毛细管柱 DB-Wax
|
-
|
1670.
|
等速升温 |
60. m/0.25 mm/0.5 μm, He, 50. C @ 2. min, 3. K/min, 230. C @ 20. min
|
Cai, J.Lin, P.Zhu, X.Su, Q.,Comparative analysis of clary sage (S. sclarea L.) oil volatiles by GC-FTIR and GC-MS,Food Chem.,2006, 99, 2, 401-407. 查看文献 |
| Normal alkane RI, 毛细管柱,等速升温 |
毛细管柱 DB-Wax
|
-
|
1688.
|
等速升温 |
60. m/0.25 mm/0.25 μm, He, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
|
Choi H.S.,Lipolytic effects of citrus peel oils and their components,J. Agric. Food Chem.,2006, 54, 9, 3254-3258. 查看文献 |